HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 44119864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 54296360 | HCID 54296360 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 44119864 | HCID 44119864 | 90% |
Reaction Steps
The methyl 2-chloro-2-deoxy-mannopyranoside (6) was dissolved in the minimum of methanol and the pH adjusted to 10 by addition of 1 molar sodium methoxide. The solution was kept for 2-5 hours at room temperature and evaported to give the 2-chloro-2-deoxy mannose in about 90% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262115 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-53771700ae9b47ed8dbb73e062ca1114 |
| Source note | uspto-grants-1981_04 |