HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Diazabicyclo(5.4.0)undec-7-ene → Acetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | Benzoylacetic acid | HCID 97045 | — |
| Product | Acetophenone | HCID 7410 | 100% |
Reaction Steps
When reacting 10 mmol of benzoylacetic acid with 20 mmol DBU at 25° C. for 3 hrs., phenyl methyl ketone was obtained in a yield of 100% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262157 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-8cf3c3dcf3114d5f9012237bdc08c5cf |
| Source note | uspto-grants-1981_04 |