HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Diazabicyclo(5.4.0)undec-7-ene → Decane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | HCID 54198982 | HCID 54198982 | — |
| Product | Decane | HCID 15600 | 45% |
Reaction Steps
By heating 5 mmol of 1,10-dodecene dicarboxylic acid with 20 mmol of DBU and 10 mmol of cuprous bromide to 340°-360° C. for 30 min. in an argon atmosphere, n-decane was obtained in a yield of 45% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262157 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-52281cf1e804418c86adfe51cb648601 |
| Source note | uspto-grants-1981_04 |