HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → HCID 20340027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 12788655 | HCID 12788655 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20340027 | HCID 20340027 | — |
Reaction Steps
To a solution of sodium (308 mg) in ethanol (40 ml) was added 5-(6-ethoxycarbonylhexyl)-1-octylhydantoin, followed by butyl bromide (1.8 g), and the solution was refluxed for 24 hours. The solvent was evaporated, water was added and the insoluble oil was extracted with ether. The washed and dried extract was evaporated to give 3-butyl-5-(6-ethoxycarbonylhexyl)-1-octyl hydantoin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04262128 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-a5a36e58513a43f7b520f355a78bc914 |
| Source note | uspto-grants-1981_04 |