Hydrochloric Acid → HCID 12788654, compound

HRID 444048Notes

Reaction equation

[CH2:1]([O:3][C:4]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][NH:12][CH:13]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[C:14]([O:16]CC)=O)=[O:5])[CH3:2].[O-:27][C:28]#[N:29].[K+].Cl>>[CH2:1]([O:3][C:4]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][N:12]1[CH:13]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[C:14](=[O:16])[NH:29][C:28]1=[O:27])=[O:5])[CH3:2]

Participants

Reactant 3

HCID 313Hydrochloric Acid

HCID 11378442Potassium cyanate

HCID 12923607HCID 12923607, compound

Product 1

HCID 12788654HCID 12788654, compound

Procedure

Ethyl 2-(6-ethoxycarbonylhexylamino)decanoate (7.4 g) was reacted with potassium cyanate and hydrochloric acid to give 1-(6-ethoxycarbonylhexyl)-5-octylhydantoin which formed colourless crystals, m.p. 68°-70° C., from light petroleum (b.p. 60°-80° C.).

Sources & evidence

ORD record: ord-1be239a5208647a08c252d0b909b0e07
Source dataset: uspto-grants-1981_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04262128

Reaction notes

Loading…