HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → HCID 53436938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Methyl 2-furoate | HCID 11902 | — |
| Product | HCID 53436938 | HCID 53436938 | 28% |
Reaction Steps
The reaction was carried out in the same manner as described in Example 21 except that 25 ml of 2-(methoxycarbonyl)furan and 0.939 g of methyl acrylate were used. Unreacted 2-(methoxycarbonyl)furan was removed from the obtained reaction solution by distillation under reduced pressure. Recrystallization of the solid residue gave 0.65 g of methyl β-(5-methoxycarbonyl-2-furyl)acrylate (4) (the yield was 28%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04263212 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-e5bec6b6a8e448a09a21ed40f06d3e30 |
| Source note | uspto-grants-1981_04 |