HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 23464483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 13013940 | HCID 13013940 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23464483 | HCID 23464483 | 100.4% |
Reaction Steps
Suspend 1.14 gm (4 mmole) of the ester of Example 23 in 60 ml of methylene chloride and add 1.035 gm of commercial m-chloroperbenzoic acid. Stir at room temperature for 45 minutes and filter. Concentrate the filtrate and separate the solids. Combine the solids to obtain the title product (yield 1.21 gm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04263207 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-54d9c542f7084a84a29c8219ea8a8dcd |
| Source note | uspto-grants-1981_04 |