HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 23464491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | HCID 23464485 | HCID 23464485 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23464491 | HCID 23464491 | — |
Reaction Steps
Dissolve 4.43 gm. of the alcohol of Step A in 100 cc. of benzene and add 1 cc (10.5 mmole) of phosphorous tribromide. Stir at room temperature for 1 hour, add water and then dilute with toluene. Wash three times with water, dry and strip to a solid residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04263207 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-6b4c7ac2cd9d459686713386e7887db3 |
| Source note | uspto-grants-1981_04 |