HRID444177

反应详情

EQUATION

反应方程式

HRID 444177 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-(4-Methylphenyl)ethyl bromide (X: X=Br) (10 g, 0.05 mole) and sodium 4-nitrophenolate (XI) (8.1 g, 0.05 mole) were added to dimethylformamide (60 ml), and the mixture was reacted at 90° C. for 5 hours. Thereafter, the reaction mixture was treated in the same manner as in Example 12 to obtain 9.5 g of 4-[2-(4-methylphenyl)ethoxy]nitrobenzene (VI) as white crystals (yield, 73.9%).

WORKUP

后处理

  1. customthe mixture was reacted at 90° C. for 5 hours
  2. additionThereafter, the reaction mixture was treated in the same manner as in Example 12
  3. customto obtain