HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 13408410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | HCID 13408409 | HCID 13408409 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13408410 | HCID 13408410 | 82% |
Reaction Steps
Reaction of 8-allyl-4-benzyloxy-7-hydroxycoumarin (12.33 g; 0.04 mole) with epichlorhydrin (25 ml) as described in Example 2(a) gave 11.97 g (82%) of product of m.p. (ethanol) 118°-121° C., νmax (mull) 1715, 1618, 1565 cm-1 (Found; C, 72.45; H, 5.53; C22H20O5 requires; C, 72.51; H, 5.53%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04263299 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-f5a0cc7fa50b408387232dac9c6765b5 |
| Source note | uspto-grants-1981_04 |