HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 136335642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | HCID 13014065 | HCID 13014065 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 136335642 | HCID 136335642 | 83% |
Reaction Steps
A mixture of 1.3 g (0.01 mole) salicylaldehyde, 2.4 g (0.01 mole) 5-hydrazino-3-trichloromethyl-1,2,4-thiadiazole, 1 ml hydrochloric acid (conc.), and 100 ml ethanol was heated 5 hours on a steam bath. Water was added and the solution cooled in a freezer several days. The resulting solid was removed by filtration to give 2.8 g (83% yield) (mp. 204°-205° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04263312 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-8c98ce918e86413b9e60e33b90b7ba2b |
| Source note | uspto-grants-1981_04 |