Salicylaldehyde → HCID 136195723, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 2.50 g (0.01 mole) 5-(1-methylhydrazino)-3-trichloromethyl-1,2,4-thiadiazole and 1.30 g (0.01 mole) salicylaldehyde was stirred. An exothermic reaction ensued and the reaction mixture warmed to 37° C. After 15 minutes ethanol was added and the solid product extracted. The product crystallized and was filtered to yield 2.15 g (61% yield) [mp. 207°-209° C. (dec)].

Provenance & Evidence