Tert-Butylamine → HCID 3055552, compound

HRID 444308Notes

Reaction equation

HRID 444308 reaction equation
[CH3:1][C:2]1[S:3][C:4]([CH:7]=[CH:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[O:15][CH2:16][CH:17]2[O:19][CH2:18]2)=[N:5][N:6]=1.[C:20]([NH2:24])([CH3:23])([CH3:22])[CH3:21]>C1(C)C=CC=CC=1>[CH3:1][C:2]1[S:3][C:4]([CH:7]=[CH:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[O:15][CH2:16][CH:17]([OH:19])[CH2:18][NH:24][C:20]([CH3:23])([CH3:22])[CH3:21])=[N:5][N:6]=1

Participants

4

Reactant 2

HCID 6385Tert-ButylamineHCID 53934759HCID 53934759, compound

Product 1

HCID 3055552HCID 3055552, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

7 g (0.025 mole) of 2-methyl-5-[2-(2,3-epoxy-propoxy)styryl]-1,3,4-thiadiazole and 2.1 g (0.028 mole) of tert.butylamine are reacted similarly to the Example relating to compound 3. 3.8 g (44% of theory) of yellow crystals, of melting point 110°-112° C., are obtained from toluene.

Sources & evidence

ORD record
ord-aff44ed8ccc149d691127d8b1a36d1e7
Source dataset
uspto-grants-1981_04
Patent number
US04263430

Reaction notes

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