HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23464884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N,N'-Bis(2,2,6,6-tetramethyl-4-piperidyl)ethylenediamine | HCID 3017249 | — |
| Reactant | 2-Chloro-4,6-bis(2,2,6,6-tetramethyl-4-piperidylamino)-1,3,5-triazine | HCID 21468017 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 23464884 | HCID 23464884 | — |
Reaction Steps
21.15 g (0.05 moles) of 2-chloro-4,6-bis(2,2,6,6-tetramethyl-4-piperidylamino)-1,3,5-triazine (prepared according to example 2A), 8.45 g (0.025 moles) of 1,2-bis-(2,2,6,6-tetramethyl-4-piperidylamino)ethane, 2 g 0.05 of sodium hydroxide and 150 ml of xylene were boiled for 16 hours under stirring. After removing the reaction solvent, the residue was washed with water, dried at 100° C./l mm and crystallized from benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04263434 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-856d3cb329ca49ea9b7764f20f130206 |
| Source note | uspto-grants-1981_04 |