HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-[(4-chlorophenyl)sulfanyl]-3-pyridinylamine → HCID 23463873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-[(4-chlorophenyl)sulfanyl]-3-pyridinylamine | HCID 2800127 | — |
| Reactant | 2,6-Dimethoxybenzoyl isocyanate | HCID 13321994 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23463873 | HCID 23463873 | — |
Reaction Steps
2,6-Dimethoxybenzoyl isocyanate (2.07 grams; 0.01 mole) and 6-(4-chlorophenylthio)-3-aminopyridine (2.37 grams; 0.01 mole) were mixed in 100 ml. of ethyl acetate and stirred at room temperature for 3 hours. Solvent was removed in vacuo and the product crystallized from hexanes-ethyl acetate, yield 0.6 gram, m.p. 172°-174° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04264605 |
| Source dataset | uspto-grants-1981_04 |
| ORD ID | ord-7f49af575b59405b9e2cb451162de747 |
| Source note | uspto-grants-1981_04 |