HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichlorosilane → HCID 66863319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichlorosilane | HCID 24811 | — |
| Reactant | HCID 19987001 | HCID 19987001 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 66863319 | HCID 66863319 | — |
Reaction Steps
The hydrosilylation reaction of Example 1 was repeated using 4.5 g of 2-allyl-5-methylthiophene in place of 2-allylthiophene, 2.5 g of anhydrous toluene, 5.0 g of trichlorosilane, and 50 mg of Platinum Catalyst. 2-(3-Trichlorosilylpropyl)-5-methylthiophene was obtained as a colorless liquid: 1H NMR (CDCl3) δ 6.60 (m, 2H); 2.88 (t, 2H, J=7.2 Hz); 2.47 (s, 3H); 1.95 (m, 2H); 1.47 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08475937B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-0b6d3a93a6e742e4a401b8660f36094f |
| Source note | uspto-grants-2013_07 |