HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67223761, compound → HCID 67224193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67223761 | HCID 67223761 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67224193 | HCID 67224193 | 100.2% |
Reaction Steps
A solution of 3-Benzyl-imidazolidine-1,5-dicarboxylic acid 1-tert-butyl ester 5-methyl ester (1.0 g, 3.12 mmol) in MeOH (20 mL) was added Pd/C (0.20 g) and stirred at room temperature under H2 for two hours. The reaction mixture was filtered through celite. The filtrate was concentrated to afford Imidazolidine-1,5-dicarboxylic acid 1-tert-butyl ester 5-methyl ester (0.72 g, xx % yield) which was used for the next step directly.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476225B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-91f298f9d8e04317b7209863e592c337 |
| Source note | uspto-grants-2013_07 |