HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67307357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 58338572 | HCID 58338572 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67307357 | HCID 67307357 | — |
Reaction Steps
Add a solution of Hydrogen Chloride in ether (1 M, 180 μL, 180.0 μmol) to a prepared solution of 4-(6-methoxy-1-(4-(2-(piperidin-1-yl)ethoxy)phenoxy)naphthalen-2-yl)thiophene-3-carbonitrile (87 mg, 179.5 μmol) in Dichloromethane (2 mL). Stir the mixture for 10 min. Concentrate the mixture to obtain the title compound (95 mg, 179 μmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476300B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-9802a598567e4531b4aea992a811f9b2 |
| Source note | uspto-grants-2013_07 |