Isoquinoline → HCID 86646593, compound

Participants

Reaction Steps

Isoquinoline (5.50 g, 42.5 mmol) was dissolved into 50 mL of anhydrous THF and ethyl chloroformate (4.47 mL, 46.8 mmol) was added slowly. The resulting pale yellow mixture was stirred at RT for 30 min. Then, the resulting precipitate was collected via filtration through a cintered glass funnel and dried under vacuum for 2 days to yield the title compound as a pale yellow solid.

Provenance & Evidence