HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86646595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 59536332 | HCID 59536332 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86646595 | HCID 86646595 | — |
Reaction Steps
To a 50 mL round-bottomed flask was added N-(4-fluorophenyl)-N-(2-methoxy-ethyl)-1H-imidazole-1-carboxamide (91 mg, 346 μmol, from step 2), acetonitrile (2 mL), methyl iodide (86 μL, 1383 μmol, Aldrich). The solution was stirred at RT for 24 h. The solvent was removed in vacuo to give the product, which was used for the next step reaction without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476297B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-add4ecea68224a3f9fdaafd2eefd4931 |
| Source note | uspto-grants-2013_07 |