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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 445374Generated: October 29, 2026

Methyl iodide → HCID 86646595, compound

https://huagongshe.com/reaction/445374

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 59536332HCID 59536332—
SolventAcetonitrileHCID 6342—
ProductHCID 86646595HCID 86646595—

Reaction Steps

To a 50 mL round-bottomed flask was added N-(4-fluorophenyl)-N-(2-methoxy-ethyl)-1H-imidazole-1-carboxamide (91 mg, 346 μmol, from step 2), acetonitrile (2 mL), methyl iodide (86 μL, 1383 μmol, Aldrich). The solution was stirred at RT for 24 h. The solvent was removed in vacuo to give the product, which was used for the next step reaction without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08476297B2
Source datasetuspto-grants-2013_07
ORD IDord-add4ecea68224a3f9fdaafd2eefd4931
Source noteuspto-grants-2013_07