HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Methyl 2-hydroxy-8-phenyloctanimidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-Hydroxy-8-phenyloctanenitrile | HCID 53925388 | — |
| Product | Methyl 2-hydroxy-8-phenyloctanimidate | HCID 66822535 | — |
Reaction Steps
A solution of 2-hydroxy-8-phenyloctanenitrile (5 g) in methanol (50 mL) was cooled to −78° C. and a stream of HCl (g) was introduced for 4 min. The mixture was stored at −10° C. for 15 h, then concentrated to yield methyl 2-hydroxy-8-phenyloctanimidate. (MH+=286).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476302B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-04d509292190443fbfc8a13bfa4d535f |
| Source note | uspto-grants-2013_07 |