HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Difluoro-2-propanol → HCID 59619636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Difluoro-2-propanol | HCID 67985 | — |
| Reactant | 5-Bromo-2-methylpyridin-3-ol | HCID 13227968 | — |
| Product | HCID 59619636 | HCID 59619636 | — |
Reaction Steps
The title compound was synthesized in a similar manner as described for stage 58.1.2 using 5-bromo-2-methyl-pyridin-3-ol (stage 189.1.2, 2.234 mmol) and 1,3-difluoro-2-propanol (Aldrich, Buchs, Switzerland, 2.68 mmol) to give the title compound as a yellow oil. (HPLC: tR 2.41 min (Method A); M+H=266, 268 MS-ES).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476294B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-481f5e935437463ea83fa4f4e1b702a6 |
| Source note | uspto-grants-2013_07 |