HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 69443055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 69442579 | HCID 69442579 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69443055 | HCID 69443055 | — |
Reaction Steps
Sulfonyl chloride (20 ml) is added to a solution of (6-benzyloxy-benzothien-2-yl) methanol (4.20 g, 15.50 mmol) in dichloromethane (40 ml). The mixture was maintained at reflux for 2 h, cooled at room temperature then concentrated under vacuum to give 4.20 g as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476455B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-5e381fb8841e4570a4c562b3ab8b372d |
| Source note | uspto-grants-2013_07 |