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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 446164Generated: October 30, 2026

Sulfuryl chloride → HCID 69443055, compound

https://huagongshe.com/reaction/446164

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSulfuryl chlorideHCID 24648—
ReactantHCID 69442579HCID 69442579—
SolventDichloromethaneHCID 6344—
ProductHCID 69443055HCID 69443055—

Reaction Steps

Sulfonyl chloride (20 ml) is added to a solution of (6-benzyloxy-benzothien-2-yl) methanol (4.20 g, 15.50 mmol) in dichloromethane (40 ml). The mixture was maintained at reflux for 2 h, cooled at room temperature then concentrated under vacuum to give 4.20 g as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08476455B2
Source datasetuspto-grants-2013_07
ORD IDord-5e381fb8841e4570a4c562b3ab8b372d
Source noteuspto-grants-2013_07