HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 86761898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 86761899 | HCID 86761899 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86761898 | HCID 86761898 | 80% |
Reaction Steps
The compound (148 mg) obtained in Example 13d was dissolved in methanol (1 mL), 4 N hydrochloric acid-dioxane (0.108 mL, 0.434 mmol) was added, and the solvent was evaporated under reduced pressure to give the title compound (127 mg; yield, 80%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476253B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-c1cd872b1f8b4a309f72c5e427f15f20 |
| Source note | uspto-grants-2013_07 |