1,4-Dioxane hydrochloride → HCID 86761906, compound

Participants

Reaction Steps

The compound (60.0 mg, 43.6 μmol) obtained in Example 41b was dissolved in dichloromethane (6 mL), a 4 N hydrochloric acid-1,4-dioxane solution (33 μL, 0.131 mmol) was added, and the mixture was stirred for 10 minutes and then concentrated under reduced pressure to give the title compound (32.4 mg; yield, 50%) as a white solid.

Provenance & Evidence