Phenethylamine → HCID 15881001, compound

HRID 446564Notes

Reaction equation

Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([O:9][CH2:10][CH3:11])=[O:8].C([CH2:19][NH2:20])C1C=CC=CC=1>>[CH3:19][NH:20][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([O:9][CH2:10][CH3:11])=[O:8]

Participants

Reactant 2

HCID 1001Phenethylamine

HCID 117544Ethyl 6-bromohexanoate

Product 1

HCID 15881001HCID 15881001, compoundYield 99.8%

Procedure

Ethyl 6-bromohexanoate (6.00 g, 26.9 mmol) and benzylmethylamine (6.52 g, 53.8 mmol) were used to give the title compound (4.65 g; yield, 99%) as a colorless oily substance according to the method described in Example 68a.

Sources & evidence

ORD record: ord-ca7c7da0287a4b67b1bd81415f5625c8
Source dataset: uspto-grants-2013_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08476253B2

Reaction notes

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