HCID 47028678, compound → HCID 86663460, compound

Participants

Reaction Steps

The compound (1.27 g, 3.78 mmol) obtained in Example 73b was dissolved in 40 mL of methanol, 100 mg of 10% palladium-carbon was added, and the mixture was stirred at room temperature under a hydrogen atmosphere for 2 hours. The reaction mixture was filtered through celite, and then the solvent of the filtrate was evaporated under reduced pressure to give the title compound (1.14 g; yield, 98%) as a colorless oily substance.

Provenance & Evidence