Toluene → HCID 66671592, compound

Participants

Reaction Steps

The compound (135 mg, 0.178 mmol) obtained in Example 73d was dissolved in 2.0 mL of dichloromethane, 2.0 mL of a 2 N hydrochloric acid-methanol solution was added, and the mixture was stirred at room temperature for 16 hours. 10 mL of toluene was added to the reaction mixture, and then the solvent was evaporated under reduced pressure to give a crude title compound.

Provenance & Evidence