HCID 86617058, compound → HCID 86617057, compound

Participants

Reaction Steps

The corresponding amine was prepared by reducing 1,2,3,7,8,9-hexachloro-4-nitrodibenzofuran with 1.8 mmol of NaSH in 5 ml of ethanol. The resulting 1,2,3,7,8,9-hexachloro-4-aminodibenzofuran was isolated by extracting with five times 30 ml of diethyl ether. The resulting solution was washed twice with 10 ml of water and dried over magnesium sulfate. Subsequently, the amine was removed from the desiccant and isolated again.

Provenance & Evidence