HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylimidazole → HCID 178480822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylimidazole | HCID 1390 | — |
| Reactant | 1-(Bromomethyl)-4-(trifluoromethyl)benzene | HCID 123062 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178480822 | HCID 178480822 | 107.4% |
Reaction Steps
By carrying out the procedure as in Step 1 of Example 10, but starting with 2 g of N-methylimidazole and 8.73 g of 4-trifluoromethylbenzyl bromide, at the reflux temperature of toluene for 2 hours, 8.4 g of 1-(4-trifluoromethylbenzyl)-3-methylimidazolium bromide are obtained in the form of an orange-yellow solid whose characteristics are the following:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08481522B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-f87c406f94b04f7da68e768f0a3eb234 |
| Source note | uspto-grants-2013_07 |