HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[2-(Pyrrolidin-1-yl)ethyl]piperazine → 4-[2-(2,4-Dichloro-benzoyl)-phenylsulfamoyl]-N-{2-oxo-2-[4-(2-pyrrolidin-1-yl-ethyl)-piperazin-1-yl]-ethyl}-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[2-(Pyrrolidin-1-yl)ethyl]piperazine | HCID 2737250 | — |
| Reactant | {4-[2-(2,4-Dichloro-benzoyl)-phenylsulfamoyl]-benzoylamino}-acetic acid | HCID 68492509 | — |
| Product | 4-[2-(2,4-Dichloro-benzoyl)-phenylsulfamoyl]-N-{2-oxo-2-[4-(2-pyrrolidin-1-yl-ethyl)-piperazin-1-yl]-ethyl}-benzamide | HCID 68577415 | — |
Reaction Steps
The title compound was prepared from {4-[2-(2,4-dichloro-benzoyl)-phenylsulfamoyl]-benzoylamino}-acetic acid and 1-(2-pyrrolidin-1-yl-ethyl)-piperazine (EMKA-Chemie) according to the method described in Example 1.1/f. MS (EI) 673.2 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08481527B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-be4ce21d0f6d4917b47584af27b37824 |
| Source note | uspto-grants-2013_07 |