HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (R)-2-AMino-N,N-diMethylpropanaMide HCl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 28165234 | HCID 28165234 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | (R)-2-AMino-N,N-diMethylpropanaMide HCl | HCID 57516590 | — |
Reaction Steps
((R)-1-Dimethylcarbamoyl-ethyl)-carbamic acid tert-butyl ester (1.1 g, 5.1 mmol) was dissolved in 26 mL of cold 4M HCl in dioxane. After 1.5 h the reaction was evaporated to provide (R)-2-amino-N,N-dimethyl-propionamide hydrochloride which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08481541B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-3f7e6a1103844b4395bf35bb14e51da2 |
| Source note | uspto-grants-2013_07 |