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HRID447913

反应详情

EQUATION

反应方程式

HRID 447913 的结构方程式

REACTANTS

反应物

2
结构：Nc1nccs1
HCID2155

2-Aminothiazole

C3H4N2S

结构：S=C(n1ccnc1)n1ccnc1
HCID80264

Thiocarbonyldiimidazole

C7H6N4S

PRODUCTS

生成物

1
结构：S=C(Nc1nccs1)n1ccnc1
HCID10750950

未命名化合物

收率 89.1%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

35 g (349.5 mmol) of 2-aminothiazole and 62.3 g (349.5 mmol) thiocarbonyldiimidazole were stirred in 1300 ml acetonitrile for a total of four days at room temperature. Filtration of the precipitate formed and drying yielded 65.5 g of light yellow solid.

WORKUP

后处理

  1. filtrationFiltration of the precipitate
  2. customformed
  3. customdrying