Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | Dronedarone Hydrochloride | HCID 219025 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | Dronedarone Sulfate | HCID 86679099 | 84% |
Reaktionsschritte
The obtained oily product was dissolved in 12 mL acetone to obtain a mixture, then 2 mL water were added to the mixture. Then, a solution of 1.1 mL concentrated sulfuric acid in 3 mL acetone was added dropwise under 10˜15° C. in about 20 min. Then, the mixture was heated to 52° C. and stirred for 1 h. The mixture was cooled by ice water bath under stirring for crystallization. After about 3.5 h later, lots of solid was precipitated. The solid obtained was filtered and dried at 50° C. under vacuum to obtain 5.5 g targeted compound. Yield: 84%, (Calculation by dronedarone hydrochloride), Purity of HPLC: 99.85%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08481763B2 |
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| Quelldatensatz | uspto-grants-2013_07 |
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| ORD ID | ord-93a30a87974b4a83ab9a7bd52df9659a |
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| Quellennotiz | uspto-grants-2013_07 |
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