Hydrochloric Acid → HCID 66994443, compound

Participants

Reaction Steps

Ether saturated with HCl (1 ml) was added at 0° C. to a solution of example 72 (0.040 g. 0.082 mmol) in THF (1 ml), and stirred for 15 min. The precipitate formed was washed with ether and dried under vacuum to afford the title compound as an off-white solid (0.040 g, 88%). M.P.: 137-140° C. MS (m/z): 483.54 (M+−2HCl).

Provenance & Evidence