Hydrochloric Acid → HCID 66995286, compound

Participants

Reaction Steps

Ether saturated with HCl (1 ml) was added at 0° C. to a solution of example 119 (0.020 g. 0.045 mmol) in THF (1 ml), and stirred for 15 min. The precipitate formed was filtered, washed with ether and dried under vacuum to afford the title compound as an off-white solid (0.012 g, 56%). M.P.: 151-153° C.

Provenance & Evidence