3-Furanol, tetrahydro- → HCID 15343685, compound

HRID 449399Notes

Reaction equation

HRID 449399 reaction equation
[OH:1][CH:2]1[CH2:6][CH2:5][O:4][CH2:3]1.Cl[C:8]([O:10][C:11]1[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][CH:12]=1)=[O:9]>>[C:8](=[O:9])([O:1][CH:2]1[CH2:6][CH2:5][O:4][CH2:3]1)[O:10][C:11]1[CH:12]=[CH:13][C:14]([N+:17]([O-:19])=[O:18])=[CH:15][CH:16]=1

Participants

3

Reactant 2

HCID 99603-Furanol, tetrahydro-HCID 821294-Nitrophenyl chloroformate

Product 1

HCID 15343685HCID 15343685, compound

Procedure

This compound was prepared by using procedures analogous to those described for the synthesis of Example 67, Step 1 starting from 3-hydroxytetrahydrofuran (Aldrich, Cat. #H59109) and p-nitrophenyl chloroformate.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-dc09170cf7b1475496d42d83175cf6e7
Source dataset
uspto-grants-2013_07
Patent number
US08481732B2

Reaction notes

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