HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trichlorobenzoic acid → 2,4,6-Trichlorobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trichlorobenzoic acid | HCID 5764 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2,4,6-Trichlorobenzoyl chloride | HCID 2733703 | 93% |
Reaction Steps
A solution of 2,4,6-trichlorobenzoic acid (1.0 g, 4.0 mmol) in SOCl2 (5 mL) was heated to reflux for 30 min under nitrogen atmosphere. The reaction was concentrated under reduced pressure to give 2,4,6-trichlorobenzoyl chloride (900 mg, 93% yield), which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486950B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-7eb410a5d5fb4b238309274731011037 |
| Source note | uspto-grants-2013_07 |