HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2,6-Dichloro-4-iodobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2,6-Dichloro-4-iodobenzoic acid | HCID 51341877 | — |
| Product | 2,6-Dichloro-4-iodobenzoyl chloride | HCID 86648958 | 100% |
Reaction Steps
A solution of 2,6-dichloro-4-iodobenzoic acid (65 mg, 0.21 mmol) in SOCl2 (3 mL) was heated to reflux under nitrogen atmosphere overnight and then cooled to room temperature. The reaction was conentrated under reduced pressure to afford 2,6-dichloro-4-iodobenzoyl chloride (70 mg, 100% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486950B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-4d56422000ae457ca41ed97b75cb9c61 |
| Source note | uspto-grants-2013_07 |