HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzoic Acid → Benzoyl chloride, 4-amino-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Benzoyl chloride, 4-amino- | HCID 177720 | 100% |
Reaction Steps
Thionyl chloride (10 ml) was added to 4-aminobenzoic acid (1.0 g, 7.29 mmol) and the solution was heated to reflux for 16 hr. Thionyl chloride was removed under vacuum to yield 4-amino-benzoyl chloride (1.13 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486962B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-9d3164fac3724e69be08b9297f716ecf |
| Source note | uspto-grants-2013_07 |