HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 3-(Methylsulfamoyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Benzoic acid, 3-(chlorosulfonyl)- | HCID 77641 | — |
| Product | 3-(Methylsulfamoyl)benzoic acid | HCID 252654 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 50A using 3-(chlorosulfonyl)benzoic acid (Aldrich) and methylamine (Aldrich). 1H NMR (300 MHz, CD3OD) δ 2.54 (s, 3 H), 7.70 (t, J=7.8 Hz, 1 H), 8.02-8.07 (m, 1 H), 8.23-8.28 (m, 1 H), 8.45 (t, J=1.9 Hz, 1 H) ppm; MS (DCI/NH3) m/z 233 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486979B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-7143b1522d124eabbe7549fcead28170 |
| Source note | uspto-grants-2013_07 |