Ammonia → HCID 44544870, compound

Participants

Role	Name	HCID	Charge
Reactant	Ammonia	HCID 222	—
Reactant	N-Hydroxynicotinimidamide	HCID 308113	—
Reactant	2,7-Dimethylpyrazolo[1,5-a]pyrimidine-6-carboxylic acid	HCID 2736303	—
Product	HCID 44544870	HCID 44544870	—

Reaction Steps

The title compound was prepared according Method C using 2,7-dimethylpyrazolo[1,5-a]pyrimidine-6-carboxylic acid (Maybridge) and N′-hydroxynicotinimidamide (Tyger). 1H NMR (300 MHz, DMSO-d6) δ2.52 (s, 3 H), 3.27 (s, 3 H), 6.77 (s, 1 H), 7.67 (ddd, J=8.0, 4.9, 0.7 Hz, 1 H), 8.48 (dt, J=8.6, 1.9 Hz, 1 H), 8.84 (dd, J=4.7, 1.7 Hz, 1 H), 9.06 (s, 1 H), 9.30 (dd, J=2.2, 0.8 Hz, 1 H), 9.30 (d, J=1.4 Hz, 1 H) ppm; MS (DCI/NH3) m/z 293 (M+H)+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08486979B2
Source dataset	uspto-grants-2013_07
ORD ID	ord-dae4b6fbcbd0466596599071aa1dfd0b
Source note	uspto-grants-2013_07