HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 67026321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 5-Bromonicotinoyl chloride | HCID 2781223 | — |
| Reactant | 3-Cyano-N-hydroxy-benzamidine | HCID 57368933 | — |
| Product | HCID 67026321 | HCID 67026321 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 4B using 3-cyano-N′-hydroxybenzimidamide and 5-bromonicotinoyl chloride (Alfa). 1H NMR (300 MHz, DMSO-d6) δ 7.67 (m, 1 H), 7.74 (m, 1 H), 8.41 (m, 1 H), 8.49 (m, 1 H), 8.64 (s, 1 H), 8.93 (s, 1 H), 9.4 (s, 1 H) ppm; MS (DCI/NH3) m/z 327 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486979B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-97105b0ef5db46c890f1340146560630 |
| Source note | uspto-grants-2013_07 |