HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 58707352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 58707373 | HCID 58707373 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 58707352 | HCID 58707352 | — |
Reaction Steps
A mixture of 2-(2,5-difluorobenzoyl)-5-methoxybenzofuran (100 mg, 0.28 mmol) and morpholine (100 mg, 1.12 mmol) in toluene (10 ml) is heated at reflux for 24 hours. Evaporation and chromatography on silicagel gives the title compound, m.p. 85-88° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08486996B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-9601fd20bbf544c7aeb7fd61b000bc9e |
| Source note | uspto-grants-2013_07 |