HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Xylyl bromide → HCID 68798725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Xylyl bromide | HCID 7721 | — |
| Reactant | 344396-17-4 | HCID 24798870 | — |
| Product | HCID 68798725 | HCID 68798725 | 20% |
Reaction Steps
This material was prepared as a 20% yield from methyl 3,5-dimethoxy-4-i-propylbenzoate and 4-methylbenzyl bromide using the same method as described in example 1 (b). 1HNMR (CDCl3, ppm): δ 1.30 (d, J=7.1 Hz, 6H), 2.31 (s, 6H), 3.02 (d, J=13.5 Hz, 2H), 3.25 (d, J=13.5 Hz, 2H), 3.52 (m, 1H), 3.71 (s, 611), 6.45 (s, 2H), 6.8-7.2 (m, 8H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08487009B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-4c1589a52e0a47c781fff6ef000d394f |
| Source note | uspto-grants-2013_07 |