HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzyl bromide → HCID 68800092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzyl bromide | HCID 68007 | — |
| Reactant | Methyl 4-isopropyl-3,5-dimethoxybenzoate | HCID 24798870 | — |
| Product | HCID 68800092 | HCID 68800092 | 70% |
Reaction Steps
This material was prepared in 70% yield from the methyl 3,5-dimethoxy-4-i-propylbenzoate and 3-fluorobenzyl bromide using the same method as described in example 1(b). 1HNMR (CDCl3, ppm): δ 1.29 (d, J=7.1 Hz, 6H), 1.85 (s, 1H), 3.07 (d, J=13.3 Hz, 2H), 3.29 (d, J=13.3 Hz, 2H), 3.56 (qint, J=7.1 Hz, 1H), 3.72 (s, 6H), 6.42 (s, 2H), 6.7-7.2 (m, 8H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08487009B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-c21b46e650c04a9292918b9547a9e501 |
| Source note | uspto-grants-2013_07 |