HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 68797239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 68796503 | HCID 68796503 | — |
| Product | HCID 68797239 | HCID 68797239 | 63% |
Reaction Steps
This compound was made from 1-(3,5-dimethoxy-4-i-propylphenyl)-2-phenylpropene (11) and BBr3 in 63% yield by the same procedure as described in example 1(c). 1HNMR (CDCl3, ppm): δ 1.42 (d, J=7.0 Hz, 6H), 2.32 (d, J=1.4 Hz, 3H), 3.49 (hept., J=7.0 Hz, 1H), 4.71 (s, 2H), 6.39 (s, 2H), 6.67 (m, 1H), 7.58-7.33 (m, 5H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08487009B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-d95e245cd1d7498889db5c5608d4fd34 |
| Source note | uspto-grants-2013_07 |