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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 451325Generated: October 30, 2026

HCID 86659598, compound → HCID 86659599, compound

https://huagongshe.com/reaction/451325

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86659598HCID 86659598—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 86659599HCID 86659599—

Reaction Steps

To a mixture of the product of Step 1 (100 mg, 0.211 mmol) in methanol was added 10% palladium on carbon (6.74 mg). The reaction mixture was stirred under an atmosphere of hydrogen (balloon) overnight then filtered. The filtrate was concentrated under vacuum to afford the title compound which was used without purification in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08487093B2
Source datasetuspto-grants-2013_07
ORD IDord-ce5c215d9e1b4ab1a38b5a94ffb3e108
Source noteuspto-grants-2013_07