HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86659598, compound → HCID 86659599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86659598 | HCID 86659598 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86659599 | HCID 86659599 | — |
Reaction Steps
To a mixture of the product of Step 1 (100 mg, 0.211 mmol) in methanol was added 10% palladium on carbon (6.74 mg). The reaction mixture was stirred under an atmosphere of hydrogen (balloon) overnight then filtered. The filtrate was concentrated under vacuum to afford the title compound which was used without purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08487093B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-ce5c215d9e1b4ab1a38b5a94ffb3e108 |
| Source note | uspto-grants-2013_07 |