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HRID451484

反应详情

EQUATION

反应方程式

HRID 451484 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NCc1cccc(B(O)O)c1
HCID3684686

3-(N-Boc-aminomethyl)phenylboronic acid

C12H18BNO4

结构：Cc1cc(Br)c2nc(N)nn2c1
HCID21464338

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(-c2cccc(CNC(=O)OC(C)(C)C)c2)c2nc(N)nn2c1
HCID67335256

未命名化合物

PROCEDURE

实验过程

Prepared in analogy to example 160b, starting from 8-bromo-6-methyl-[1,2,4]triazolo[1,5-a]pyridin-2-amine and 3-((tert-butoxycarbonylamino)methyl)phenylboronic acid. The title compound was obtained as an off-white solid (yield: 99%) after precipitation from diethyl ether. MS ISP (m/e): 354.4 (80) [(M+H)+], 298.4 (100), 237.2 (99).

WORKUP

后处理

  1. customPrepared in analogy to example 160b