Hydrochloric Acid → HCID 67342611, compound

Participants

Reaction Steps

To a solution tert-butyl 1-(6-methylpyridazin-4-yl)piperidin-4-ylcarbamate (2.14 g, 7.32 mmol) in dichloromethane (36 mL) was added HCl (2 M in diethylether, 18.3 mL, 36.6 mmol) and the reaction mixture was stirred at room temperature for 24 hours. The mixture was then filtered and the white precipitate was washed with dichloromethane and diethylether and dried to afford the title compound (2.35 g, 82%) as a white solid.

Provenance & Evidence